Monolithic silicas in separation science : concepts, syntheses, characterization, modeling and applications /
Edited by the experts and pioneers in the field, this is the first monograph to cover the topic, containing the must-have information hitherto only scattered among journals. Clearly divided into sections on preparation, characterization and modeling, and applications, this is essential reading for c...
Άλλοι συγγραφείς: | , , |
---|---|
Μορφή: | Ηλ. βιβλίο |
Γλώσσα: | English |
Έκδοση: |
Weinheim :
Wiley-VCH,
2011.
|
Θέματα: | |
Διαθέσιμο Online: | Full Text via HEAL-Link |
Πίνακας περιεχομένων:
- Monolithic Silicas in Separation Science; Contents; Preface; List of Contributors; 1: The Basic Idea and the Drivers; 1.1: Definitions; 1.2: Monoliths as Heterogeneous Catalysts; 1.3: Monoliths in Chromatographic Separations; 1.4: Conclusion and Perspectives; References; Part One: Preparation; 2: Synthesis Concepts and Preparation of Silica Monoliths; 3: Preparation and Properties of Various Types of Monolithic Silica Stationary Phases for Reversed-Phase, Hydrophilic Interaction, and Ion-Exchange Chromatography Based on Polymer-Coated Materials; Part Two: Characterization and Modeling.
- 4: Characterization of the Pore Structure of Monolithic Silicas5: Microscopic Characterizations; 6: Modeling Chromatographic Band Broadening in Monolithic Columns; 7: Comparison of the Performance of Particle-Packed and Monolithic Columns in High-Performance Liquid Chromatography; 7.1: Introduction; 7.2: Basic Columns Properties; 7.3: Comparison of the Through-Pore Structures and Related Properties; 7.4: Thermodynamic Properties; 7.5: Kinetic Properties and Column Efficiency; 7.6: Conclusions; Part Three: Applications.
- 8: Quantitative Structure-Retention Relationships in Studies of Monolithic Materials9: Performance of Silica Monoliths for Basic Compounds. Silanol Activity; 10: Quality Control of Drugs; 11: Monolithic Stationary Phases for Fast Ion Chromatography; 12: Monolithic Chiral Stationary Phases for Liquid-Phase Enantioseparation Techniques; 13: High-Speed and High-Efficiency Separations by Utilizing Monolithic Silica Capillary Columns; 14: Silica Monolithic Columns and Mass Spectrometry; 15: Silica Monoliths for Small-Scale Purification of Drug-Discovery Compounds.
- 16: Monolithic Silica Columns in Multidimensional LC-MS for Proteomics and Peptidomics17: Silica Monoliths in Solid-Phase Extraction and Solid-Phase Microextraction; 17.1: Introduction; 17.2: Extraction Process; 17.3: Extraction Platforms; 17.4: Applications; 17.5: Conclusion and Outlook; References; Index.