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06286nam a2200805 4500 |
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ocn818985754 |
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OCoLC |
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20170124071357.2 |
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121120s2013 enk ob 001 0 eng |
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|a 2012047055
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|a MAIN
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1 |
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|a Motzfeldt, K.
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|a High temperature experiments in chemistry and materials science /
|c Ketil Motzfeldt.
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| 264 |
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|a Chichester, West Sussex, United Kingdom :
|b Wiley.,
|c 2013.
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| 300 |
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|a 1 online resource.
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| 336 |
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|a text
|2 rdacontent
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| 337 |
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|a computer
|2 rdamedia
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| 338 |
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|a online resource
|2 rdacarrier
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|a data file
|2 rda
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| 520 |
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|a "The present text is centred around some central topics within high-temperature chemistry. It concerns the control and measurement of the basic properties"--
|c Provided by publisher.
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| 504 |
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|a Includes bibliographical references and index.
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| 500 |
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|a Machine generated contents note: Foreword vii Preface ix 1 Introduction to High-Temperature Research 1 2 Basic Design of Laboratory Furnaces 11 3 Temperature Measurements 55 4 Radiation Pyrometry 93 5 Refractory Materials in the Laboratory 129 6 Vacuum in Theory and Practice 177 7 High-Temperature Furnaces and Thermobalances 229 8 The Summing Up 267 Author Index 317 Subject Index 000 .
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| 588 |
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|a Description based on print version record and CIP data provided by publisher.
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0 |
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|a High Temperature Experiments in Chemistry and Materials Science; Contents; Foreword; Preface; Acknowledgements; 1 Introduction to High Temperature Research; Preamble; 1.1 The Basis of It All; 1.1.1 Photosynthesis; 1.1.2 The Role of Carbon; 1.2 High Temperatures; 1.2.1 Chemistry at Ambient Temperatures; 1.2.2 Chemistry at High Temperatures; 1.2.3 The Nitrogen Industry; 1.2.4 Iron and Steel; 1.3 Carbothermal Silicon and Aluminium; 1.3.1 Ferrosilicon and Silicon Metal; 1.3.2 The First Laboratory Furnace; 1.3.3 Carbothermal Aluminium; 1.3.4 More Laboratory Furnaces.
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|a 1.3.5 A Note on Chemical Thermodynamics1.4 Summary of Contents; Select Bibliography; 2 Basic Design of Laboratory Furnaces; Preamble; 2.1 Methods of Heating; 2.2 Materials; 2.2.1 Electric Conductors or Resistors; 2.2.2 Insulating Materials; 2.3 Basic Furnace Design; 2.3.1 Obtaining a Uniform Temperature; 2.3.2 Base Metal Wire; 2.3.3 The Stand and Auxiliaries; 2.3.4 Silicon Carbide; 2.3.5 Molybdenum Disilicide; 2.3.6 Oxide Resistors; 2.3.7 Noble Metals; 2.3.8 Molybdenum Wire; 2.3.9 Graphite; 2.4 Induction Heating; 2.4.1 Elementary Principles; 2.4.2 High Frequency Generators.
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|a 2.4.3 Some Laboratory Applications2.5 Power Input, Insulation and Cooling; 2.5.1 Power and Temperature; 2.5.2 Thermal Insulation; 2.5.3 Water Cooling; 2.6 Temperature Control; 2.6.1 Elementary Principles and Two-Position Control; 2.6.2 PID Control; 2.6.3 Power Regulators; 2.6.4 Sensing Elements for Control; 2.7 Electric Connections and Circuits; 2.7.1 General Rules; 2.7.2 Current-Carrying Capacity of Insulated Copper Wire; 2.7.3 Fail-Safe Protection Devices; References; 3 Temperature Measurements; Preamble; 3.1 Fundamentals of Temperature Measurement; 3.1.1 The Concept of Temperature.
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|a 3.1.2 The Thermodynamic Temperature Scale3.1.3 The Gas Thermometer and the Practical Temperature Scale; 3.1.4 History of the International Temperature Scales; 3.1.5 The International Temperature Scale of 1990 (ITS-90); 3.2 'Low-Temperature' Thermometers; 3.2.1 Liquid-in-Glass Thermometers; 3.2.2 Bimetallic Thermometers and Thermostats; 3.2.3 Semiconductor-Based Thermometers; 3.2.4 Resistance Thermometers; 3.3 Thermocouples; 3.3.1 Principles of Thermoelectricity; 3.3.2 Thermocouple Materials; 3.3.3 Base-Metal Thermocouples; 3.3.4 Noble-Metal Thermocouples.
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|a 3.3.5 Insulating Materials and Installation3.3.6 MIMS Thermocouples; 3.3.7 Thermocouples for Very High Temperatures; 3.3.8 The Cold Junction; 3.3.9 Extension and Compensating Wires; 3.3.10 Control and Calibration; 3.3.11 The Measurement of Small e.m.f.'s; 3.3.12 More about Thermoelectricity; 3.4 Literature; References; 4 Radiation Pyrometry; Preamble; 4.1 Basic Principles; 4.1.1 The Nature of Heat and Radiation; 4.1.2 Formation and Propagation; 4.1.3 The Concept of the Black Body; 4.1.4 Emission, Absorbtion and Kirchhoff's Law; 4.1.5 Total Radiation, Stefan and Boltzmann.
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| 650 |
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|a High temperature chemistry
|x Experiments.
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| 650 |
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|a Materials at high temperatures
|x Experiments.
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| 650 |
|
7 |
|a SCIENCE / Chemistry / Physical & Theoretical.
|2 bisacsh
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| 650 |
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4 |
|a SCIENCE
|x Chemistry
|x Physical & Theoretical.
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| 650 |
|
7 |
|a Science.
|2 fast
|0 (OCoLC)fst01108176
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| 655 |
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|a Electronic books.
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| 655 |
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7 |
|a Electronic books.
|2 local
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| 776 |
0 |
8 |
|i Print version:
|a Motzfeldt, Keith.
|t High temperature experiments in chemistry and materials science
|d Chichester, West Sussex, United Kingdom : John Wiley & Sons Inc., 2013
|z 9781118457696
|w (DLC) 2012034399
|
| 856 |
4 |
0 |
|u https://doi.org/10.1002/9781118457795
|z Full Text via HEAL-Link
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| 994 |
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|a 92
|b DG1
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